Detection of the illegal use of ethinylestradiol in cattle urine by gas chromatography-mass spectrometry

E Daeseleire, A De Guesquière, C Van Peteghem

    Onderzoeksoutput: Bijdrage aan tijdschriftA1: Web of Science-artikelpeer review

    Uittreksel

    A method for the detection of ethinylestradiol in cattle urine is described, based on enzymic hydrolysis of the sample, clean-up by means of disposable octadecyl and amino solid-phase extraction columns, fractionation by reversed-phase high-performance liquid chromatography, and detection by gas chromatography-mass spectrometry (selected-ion monitoring). Identification is based on both gas chromatographic and mass spectrometric data. The method has been tested on urine samples for a collaborative study and all the results found were correct.
    Oorspronkelijke taalEngels
    TijdschriftJournal of Chromatography A
    Volume564
    Exemplaarnummer2
    Pagina's (van-tot)469-75
    Aantal pagina’s7
    ISSN0021-9673
    PublicatiestatusGepubliceerd - 1991

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