Multi-Class UHPLC-MS/MS Method for Plant Toxins and Cyanotoxins in Food Supplements and Application for Belgian Market Samples (#)

E Van Pamel, J Henrottin, C Van Poucke, N Gillard, E Daeseleire

Onderzoeksoutput: Bijdrage aan tijdschriftArtikelpeer review

Uittreksel

The presence of plant toxins and/or cyanotoxins in food supplements implies consumer health risks. Therefore, a targeted ultra-high performance liquid chromatographic-tandem mass spectrometric method to detect/quantify 25 toxins simultaneously in food supplement formulations was developed and validated. Full validation for tablets/powders and secondary validation for a liquid and soft gel capsule indicated that most compounds were efficiently extracted (>= 75%), while others were only partly extracted (18-61%). Trueness was fulfilled (70-120%), with some exceptions (mostly at the lowest validation level). Intralaboratory repeatability, intra- and interlaboratory reproducibility values of
Oorspronkelijke taalEngels
TijdschriftPLANTA MEDICA
Volume87
Exemplaarnummer12/13
Pagina's (van-tot)1069-1079
Aantal pagina’s11
ISSN0032-0943
DOI's
PublicatiestatusGepubliceerd - jun-2021

Dit citeren