Validation of the βeta-s.t.a.r. Combo for fast screening of raw milk on the presence of ß-lactam antibiotics and tetracyclines

Wim Reybroeck; Sigrid Ooghe

Validation of the βeta-s.t.a.r. Combo for fast screening of raw milk on the presence of ß-lactam antibiotics and tetracyclines

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The 5-minute test ßeta-s.t.a.r. Combo (Neogen Corporation, Lansing, MI) was validated at ILVO-T&V according to Commission Decision 2002/657/EC and the CRL Guidelines for the validation of screening methods by determination of the test specificity, detection capabilities and test robustness.
In the validation study the test showed to be very specific as a real interference was only caused by clavulanic acid at 700 µg/kg and above. The ßeta-s.t.a.r. Combo detects all ß-lactams and tetracyclines with a MRL in milk at their respective MRL except for cefalexin and desfuroylceftiofur.
Positive results for milk with an abnormal composition/quality should be considered with caution since interferences (false positive results) were observed. Retesting of initially positive milk samples could be a recommendation.

Oorspronkelijke taal	Engels
Titel	Residues of veterinary drugs in food : Proceedings of the EuroResidue VII Conference, Egmond aan Zee, The Netherlands, 14-16 May 2012
Editors	Robert Schilt
Aantal pagina’s	6
Volume	2
Publicatiedatum	2012
Pagina's	557-562
ISBN van geprinte versie	978-94-6173-318-4
Publicatiestatus	Gepubliceerd - 2012
Evenement	EuroResidue VII Conference on Residues of Veterinary Drugs in Food - Egmond aan Zee, Egmond aan Zee, Nederland Duur: 14-mei-2012 → 16-mei-2012

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Manuscript EuroResidue Beta star combo ref!!Submitted manuscript, 390 KB

VALIDATIEANTIBIO: Validatie van screeningstesten voor antibioticaresiduen voor kitproducenten
Heyndrickx, M. (Projectverantwoordelijke), Ooghe, S. (Projectbegeleider) & Reybroeck, W. (Voormalig Projectbegeleider)
1/01/10 → …
Project: Onderzoek

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title = "Validation of the βeta-s.t.a.r. Combo for fast screening of raw milk on the presence of {\ss}-lactam antibiotics and tetracyclines",

abstract = "The 5-minute test {\ss}eta-s.t.a.r. Combo (Neogen Corporation, Lansing, MI) was validated at ILVO-T&V according to Commission Decision 2002/657/EC and the CRL Guidelines for the validation of screening methods by determination of the test specificity, detection capabilities and test robustness. In the validation study the test showed to be very specific as a real interference was only caused by clavulanic acid at 700 µg/kg and above. The {\ss}eta-s.t.a.r. Combo detects all {\ss}-lactams and tetracyclines with a MRL in milk at their respective MRL except for cefalexin and desfuroylceftiofur. Positive results for milk with an abnormal composition/quality should be considered with caution since interferences (false positive results) were observed. Retesting of initially positive milk samples could be a recommendation. ",

author = "Wim Reybroeck and Sigrid Ooghe",

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language = "English",

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volume = "2",

pages = "557--562",

editor = "Schilt, {Robert }",

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note = "EuroResidue VII Conference on Residues of Veterinary Drugs in Food ; Conference date: 14-05-2012 Through 16-05-2012",

}

Reybroeck, W & Ooghe, S 2012, Validation of the βeta-s.t.a.r. Combo for fast screening of raw milk on the presence of ß-lactam antibiotics and tetracyclines. in R Schilt (ed.), Residues of veterinary drugs in food: Proceedings of the EuroResidue VII Conference, Egmond aan Zee, The Netherlands, 14-16 May 2012. vol. 2, blz. 557-562, EuroResidue VII Conference on Residues of Veterinary Drugs in Food, Egmond aan Zee, Nederland, 14/05/12.

Validation of the βeta-s.t.a.r. Combo for fast screening of raw milk on the presence of ß-lactam antibiotics and tetracyclines. / Reybroeck, Wim; Ooghe, Sigrid.
Residues of veterinary drugs in food: Proceedings of the EuroResidue VII Conference, Egmond aan Zee, The Netherlands, 14-16 May 2012. ed. / Robert Schilt. Vol. 2 2012. blz. 557-562.

Onderzoeksoutput: Hoofdstuk in Boek/Rapport/Congresprocedure › C1: Artikels in proceedings van wetenschappelijke congressen, die niet inbegrepen zijn in A1, A2, A3 of P1

TY - CHAP

T1 - Validation of the βeta-s.t.a.r. Combo for fast screening of raw milk on the presence of ß-lactam antibiotics and tetracyclines

AU - Reybroeck, Wim

AU - Ooghe, Sigrid

PY - 2012

Y1 - 2012

N2 - The 5-minute test ßeta-s.t.a.r. Combo (Neogen Corporation, Lansing, MI) was validated at ILVO-T&V according to Commission Decision 2002/657/EC and the CRL Guidelines for the validation of screening methods by determination of the test specificity, detection capabilities and test robustness. In the validation study the test showed to be very specific as a real interference was only caused by clavulanic acid at 700 µg/kg and above. The ßeta-s.t.a.r. Combo detects all ß-lactams and tetracyclines with a MRL in milk at their respective MRL except for cefalexin and desfuroylceftiofur. Positive results for milk with an abnormal composition/quality should be considered with caution since interferences (false positive results) were observed. Retesting of initially positive milk samples could be a recommendation.

AB - The 5-minute test ßeta-s.t.a.r. Combo (Neogen Corporation, Lansing, MI) was validated at ILVO-T&V according to Commission Decision 2002/657/EC and the CRL Guidelines for the validation of screening methods by determination of the test specificity, detection capabilities and test robustness. In the validation study the test showed to be very specific as a real interference was only caused by clavulanic acid at 700 µg/kg and above. The ßeta-s.t.a.r. Combo detects all ß-lactams and tetracyclines with a MRL in milk at their respective MRL except for cefalexin and desfuroylceftiofur. Positive results for milk with an abnormal composition/quality should be considered with caution since interferences (false positive results) were observed. Retesting of initially positive milk samples could be a recommendation.

M3 - C1: Articles in proceedings

SN - 978-94-6173-318-4

VL - 2

SP - 557

EP - 562

BT - Residues of veterinary drugs in food

A2 - Schilt, Robert

T2 - EuroResidue VII Conference on Residues of Veterinary Drugs in Food

Y2 - 14 May 2012 through 16 May 2012

ER -

Validation of the βeta-s.t.a.r. Combo for fast screening of raw milk on the presence of ß-lactam antibiotics and tetracyclines

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VALIDATIEANTIBIO: Validatie van screeningstesten voor antibioticaresiduen voor kitproducenten

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